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An Old Reaction Revisited
June 30, 2015Chemoselective Reductive Amination of Carbonyl Compounds for the Synthesis of Tertiary Amines Using SnCl2·2H2O/PMHS/MeOH A new protocol for a reductive amination…
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Not So Easy
June 23, 2015Synthesis of Heteroaryl Sulfonamides from Organozinc Reagents and 2,4,6-Trichlorophenyl Chlorosulfate Access to sulfonated heterocycles using zincates and the reagent TCPC. It…
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New CO-nditions
June 10, 2015Aminocarbonylation of Aryl Tosylates to Carboxamides Generation of aromatic amides using CO, amines and aryl tosylates as coupling substrates. This is…
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Bubbles
June 8, 2015Oxalyl Chloride as a Practical Carbon Monoxide Source for Carbonylation Reactions A new way to get a balloon filled with CO…
Read MoreIpso Facto
June 1, 2015Ipso-Borylation of Aryl Ethers via Ni-Catalyzed C–OMe Cleavage The OMe moiety used as entry point for the borylation of aryl and…
Read MoreImpressive, Most Impressive
May 27, 2015Practical olefin hydroamination with nitroarenes A new, powerful method to generate quaternary amines without using expensive catalysts. Baran has done it…
Read MoreGotcha!
May 21, 2015In Situ Generation of Difluoromethyl Diazomethane for [3+2] Cycloadditions with Alkynes Safe preparation of an elusive reagent, difluoromethyl diazomethane, and its…
Read MoreWorking on the Edge
May 19, 2015Metal-Free, Regio- and Stereoselective Synthesis of Linear (E)?Allylic Compounds Using C, N, O, and S Nucleophiles Using terminal alkenes to prepare…
Read MoreSuzuki on the Rocks
May 14, 2015Palladium-Catalyzed, Ligand-Free Suzuki Reaction in Water Using Aryl Fluorosulfates Not only we can couple the most exotic moieties, we can do…
Read MoreCatalysis for Amides
May 4, 2015Catalytic Chemical Amide Synthesis at Room Temperature: One More Step Toward Peptide Synthesis An uncommon use of a boronic acid: as…
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